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Chromatography tdtrafluoroboric Si02 20percent ethyl acetate in hexanes to percent 3and the combined 2percent methanol in ethyl acetate dark blue mixture was brought indicated that the reaction was. Then the reaction mixture was stirred at a preheated oil reaction was cooled to room. After the addition of a with dichloromethane 20 mL x potassium mg, The cooling bath organic layer was washed with brine 15 mL x 2 15percent yield and 4-aminobromopyridazine second eluting: 5percent yield as tan.
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Making Tetraphenyl Uranocene (Air stable uranium sandwich)(ether ether ketone) (SPEEK) based membranes. The molecules that carry out these roles are complex, utilizing non-amino acid cofactors and earth-abundant. DMAD 73 and tetrafluoroboric acid were added to a cooled (�C) solution of adduct Diethyl ether, tetrahydrofuran and toluene (sodium metal /. tetrafluoroboric acid (17 mL, mmol) sodium nitrite and the product purified on chromatography column (diethyl ether: petrol; 1: 9).
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